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    LIQUID GAS SEPARATION

    Presented by:

    Mara Catalina Monroy Muoz

    Carlos David Perez Ros

    Marlon Alfredo Zorro O.

    Presented to:

    M.Sc Nicols Santos Santos

    Escuela de Ingeniera de Petrleos

    Universidad Industrial de Santander

    2016

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    OUTLINE

    Introduction

    Separators Principles.

    Separation Functions.

    Separator Types

    Vessel Internals

    Potential Operating Problems

    Separator Design

    Conclusions

    Bibliography

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    INTRODUCTION

    WELL FLUID

    Gas

    Oil

    Water

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    SEPARATORS

    1. Inlet Stream: Changes in

    the amount of momentum andcentrifugal force.

    2. Gravity Settl ing Section:

    Stokes Law, Drag Force,

    Gravity Force.

    3. Mist Extractor: Drag

    Force, Coalescence and

    Gravity Force

    4. Liquid Collection Section:

    Retention Time.

    Source:ARNOLD, Ken. Surface Production Operation. Vol

    1.2.

    3.

    4.

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    =1,488

    ,

    18 =

    This law also defines the relationship between particle size and th

    of gravitational settling.

    STOKES LAW

    SEPARATORS PRINCIPLES

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    It is this force that removes the liquid droplets contained in the g

    =

    2

    Where:

    FD drag force, lbf (N),

    CD drag coefficient,

    A cross-sectional area of the droplet, ft2 (m2),

    density of the continuous phase, lb/ft3 (kg/m3),

    Vt terminal (settling velocity) of the droplet, ft/sec (m/sec),

    g gravitational constant, 32.2 lbmft/lbf sec2 (m/sec2).

    DRAG FORCE

    SEPARATORS PRINCIPLES

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    If the flow around the droplet were laminar, then Stokegovern and where Re = Reynolds number is less two.

    =24

    =1.7810()

    Unfortunately, for production facility designs it can be shownlaw does not govern.

    34,0Re

    3

    Re

    2421 DC

    21

    0119,0

    D

    m

    g

    gL

    tC

    dV

    DRAG FORCE

    SEPARATORS PRINCIPLES

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    SEPARATORS PRINCIPLES

    Mark Bothamley,

    DROPLET SIZE

    Gravity settling section collectsdrops to 140 m higher.

    Extractor generates fogdroplets coalescence between10-140 m.

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    SEPARATORS PRINCIPLES

    =

    API Gravity

    Tiempo de

    retencin (min)

    35+ 0.5-1

    30 2

    25 3

    20- 4+

    For the liquid and gas separator pressure equilibreached, a liquid storage is required. This is defined as "retentio

    RETENTION TIME

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    Source

    SEPARATORS PRINCIPLES

    CHANGES IN THE AMOUNT OF MOMENTUM

    CENTRIFUGAL FORCE

    COALESCENCE

    GRAVITY FORCE

    OTHERS

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    SEPARATORS FUNCTION

    Source: w

    It makes the first phases separation between

    hydrocarbons.

    Enhanced the separation process through the

    collection of liquid particles trapped in the gas

    phase and the gas particles trapped in liquid

    phase.

    Release the trapped gas phase in the liquid

    phase.

    Downloaded separately the liquid and gas phase.

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    SEPARATION TYPES

    HORIZONTALSEPARATORS

    VERTICALSEPARATORS

    SPHERICALSEPARATORS

    OTHERS

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    HORIZONTAL SEPARATORS

    Source:ARNOLD, Ken. Surface Production Operation. Volumes I & III. Chapter 4. 2008.

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    HORIZONTAL SEPARATORS

    Source: BOLLAND. Separadores lquidos, gases y slidos. El Medanito, Argentina.

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    Efficient handling and processing of high volumliquid.

    Suitable for separating emulsions.

    Easy maintenance and transportation.

    Does not handle solids

    Requires more space.

    Turbulence limitations.

    Variables rates.

    HORIZONTAL SEPARATORS

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    Source: GPSA. Engineering Data Book. FPS Version. Volumes I & II. Sections 1 - 26. Chapter 7. 2004.

    VERTICAL SEPARATORS

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    Source: ARRIETA, Mario. Estaciones de flujo.

    VERTICAL SEPARATORS

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    Efficient solids control.

    Less likely to return liquid to gas flow.

    Good for low GOR.

    Requires less space.

    Difficult maintenance.

    Little contact area between the phases.

    Transport limitations.

    VERTICAL SEPARATORS

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    Type QGas and

    Liquid

    Foamy

    crude

    Gas /Oil

    Easy

    operation

    and

    maintenan

    ce

    Manageme

    nt of solids Installation

    area

    Abso

    turb

    Horizontal

    Vertical

    SCREENING

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    Source:ARNOLD, Ken. Surface Production Operation. Volumes I & III. Chapter 4. 2008.

    SPHERICAL SEPARATORS

    HORIZONTAL FILTER

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    Solids

    Liquid

    coalesced

    Source:ARNOLD, Ken. Surface Production Operation. Volumes I & III. Chapter 4. 2008.

    HORIZONTAL FILTER

    SEPARATORS

    HORIZONTAL FILTER

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    APP

    LICATIONS

    Entries compressor stations.

    High GOR.

    Removal of particles larger than 2 microns.

    Pressure drop normal of 1 2 psi.

    10 psi pressure drop criteria is used for filter change out.

    HORIZONTAL FILTER

    SEPARATORS

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    OTHERS

    SLUG CATCHER

    A particular separator design

    able to handle large liquid

    volumes at irregular intervals.

    Source:ARNOLD, Ken. Surface Production O2008.

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    SLUG CATCHER

    OTHERS

    Source: Cat

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    OTHERS

    SCRUBBER

    Vessel designed to handle

    streams with high gas to liquid

    ratios, usually have a small

    liquid collection section.

    Source: CAMPBELL. Gas Conditioning and processing Vo

    O S

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    OTHERS

    SCRUBBER

    Source: Catlogo Exterran.

    OTHERS

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    OTHERS

    SCRUBBER

    BER

    Source: CarUSA. Gas Scrubber.

    OTHERS

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    OTHERS

    DOUBLE-BARRELHORIZONTAL SEPARATORS

    CENTRIFUSEPARATO

    Source:ARNOLD, Ken. Surface Production Operation. Volumes I & III. Chapter 4. 2008.

    OTHERS

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    THREE PHASE SEPARATORS

    OTHERS

    Source: http://www.fenixchemtech.in/pdf_cat/intsep.pdf

    VESSEL INTERNALS

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    SEPARATORS ALL HAVE IN COMMON FOURSECTIONS:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    VESSEL INTERNALS

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    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Vertical separator schematic

    Mist Extractor

    Inlet Diverter

    Liquid

    Collection

    section

    Gravity settling

    section.

    Gas Out

    Pressure

    Control Valve

    Inlet

    Gas-Liquid Interface

    Liquid Out

    Level Control Valve

    VESSEL INTERNALS

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    Element that abruptly changes the

    direction of flow, causing the release of

    gas.

    Reduce the momentum.

    Perform an anitial separation.

    THE INLET DEVICE

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operation

    Baffle plates

    VESSEL INTERNALS

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    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Three views of an example centrifugal inlet diverter

    VESSEL INTERNALS

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    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production OperationsSource:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Elbow inlet diverter

    Centrifugal inlet diverters. (Top) C

    Tangential raceway.

    VESSEL INTERNALS

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    A reduction in flow rate of the

    gas stream occurs, allowing

    suspended liquid droplets fall by

    gravity.

    GAS GRAVITY SEPARATION SECTION

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operatio

    Third Edition.

    VESSEL INTERNALS

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    LIQUID COLLECTION SECTION

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    VESSEL INTERNALS

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    This device generates numerous

    changes in the flow direction of the gas,

    causing the liquid droplets ( less than

    100 microns ) are caught by

    coalescing elements and fall bygravity.

    MIST EXTRACTION SECTION:

    VESSEL INTERNALS

    Source: ARNOLD, K. Surface Production Operations

    VESSEL INTERNALS

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    BAFFLES:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition. Source:ARNOLD, K. Surface Production Operations. Vo

    Typical vane-type mist extractor/ eliminator Vane-type element with corrugated

    drainage trays

    VESSEL INTERNALS

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    BAFFLES:

    VESSEL INTERNALS

    Source: ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition. Source: ARNOLD, K. Surface Production Operations. Vo

    Cutaway view of a vertical separator fitted with a vane- type

    mist extractor.

    Cutaway view of a horizontal separator fit

    mist extractor.

    VESSEL INTERNALS

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    BAFFLES:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    A vane-type mist extractor made from angle iron

    VESSEL INTERNALS

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    BAFFLES:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    An arch plate-type mist extractor

    VESSEL INTERNALS

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    WIRE MESH:

    VESSEL INTERNALS

    Source: ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Example wire-mesh mist extractor.

    VESSEL INTERNALS

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    WIRE MESH:

    VESSEL INTERNALS

    Vertical separators fitted with wire-mesh pads supported by support rings

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    VESSEL INTERNALS

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    WIRE MESH:

    VESSEL INTERNALS

    Horizontal separator fitted with wire-mesh pads supported by a frame.

    Source: ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    VESSEL INTERNALS

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    OTHER CONFIGURATIONS:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Centrifugal mist extractor Vertical separator fitted with a c

    VESSEL INTERNALS

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    OTHER CONFIGURATIONS:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    A coalescing pack mist extractor

    VESSEL INTERNALS

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    WAVE BREAKERS:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Three-dimensional view of a horizontal separator fitted with an inlet diverter, defoaming e

    And wave breaker

    VESSEL INTERNALS

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    DEFOAMING PLATES:

    VESSEL INTERNALS

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Defoaming plates

    VESSEL INTERNALS

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    VORTEX BREAKER:

    SS S

    Vortex breaker Typical vortex breakers

    Source: ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    VESSEL INTERNALS

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    SAND JETS AND DRAINS:

    Source:ARNOLD, K. Surface Production Operations. Vol.1. Chapter 3 Third Edition.

    Schematic of a horizontal separator fitted with sand jets and inverted trou

    VESSEL INTERNALS

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    EXTERNAL ACCESSORIOS:

    SAFETY RELIEF VALVE

    CONTROL VALVES BACKPRESSURE

    FULL CONTROL VALVES

    POTENTIAL OPERATINGPROBLEMS

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    PROBLEMS

    FOAMY CRUDE

    CO2 > 1-2%

    1.Mechanical control of liquid level isaggravated.

    2. Foam has a large volume-to-weight r

    3. An uncontrolled foam bank.

    POTENTIAL OPERATINGPROBLEMS

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    PARAFAFFIN SAND

    Coalescing plates in the liquid section

    and mesh pad mist extractors in the

    gas section are particularly prone to

    plugging by accumulations of paraffin.

    Cutout of valve trim.

    Plugging of separator i

    Accumulation in the

    separator.

    PROBLEMS

    POTENTIAL OPERATINGPROBLEMS

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    Source:ARNOLD, Ken. Surface Production Operation. Volumes I & III. Chapter 4. 2008.

    Vertical separator with a pressure

    containing cone bottom used to

    collect solids.

    Vertical separator fit te

    internal cone bottom

    equalizing l in

    PROBLEMS

    POTENTIAL OPERATINGPROBLEMS

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    LIQUID CARRYOVER GAS BLOWY

    Occurs when free liquid escapes

    with the gas phase.

    Occurs when free g

    with the liquid phase

    an indication of low

    vortexing, or level contr

    PROBLEMS

    POTENTIAL OPERATINGPROBLEMS

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    LIQUID SLUGS

    Two-phase flow lines and pipelines tend to accumulate liquids

    low spots in the lines. When the level of liquid in these low sp

    rises high enough to block the gas flow, then the gas will push

    liquid along the line as a slug.

    PROBLEMS

    DESIGN THEORY

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    In the design of separators, it must be determined initially the dra

    performing a process of trial and error with equations settl

    Reynold's number and drag coefficient.

    COEFFICIENT OF DRAG

    CD =24

    3

    . 0.34

    HORIZONTAL SEPARATORSIZING

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    SIZING

    GAS CAPACITY CONSTRAINT:

    LIQUID CAPACITY CONSTRAINT:

    21

    420

    m

    D

    gl

    gg

    effd

    C

    P

    TZQdL

    7,0

    2 lreff

    QtLd

    Where:

    d= Inches

    Leff= ft

    Lss= ft

    T= R

    P= psia

    Qg= MMscf

    Ql= Bpd

    p= lb/ft^3dm= Micro

    tr= Minutes

    Cd= Drag c

    Z= Gas com

    HORIZONTAL SEPARATORSIZING

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    SELECTION:

    SIZING

    d

    LSR SS

    12

    d= InchesLss= ft

    SR= DimensionSlenderness Ratio=

    d (in) Gas Leff (ft) Liquid Leff

    (ft)

    Lss S

    16

    20

    .

    .

    36

    42

    VERTICAL SEPARATORSIZING

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    SIZING

    GAS CAPACITY CONSTRAINT:

    LIQUID CAPACITY CONSTRAINT:

    = 5040

    =

    0,12

    12

    76h

    LSS

    12

    40

    dhLSS

    For diameters < 36

    For diameters < 36

    VERTICAL SEPARATORSIZING

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    SELECTION:

    dLSR SS12Slenderness Ratio=

    d= Inches

    Lss= ftSR= Dimensionless

    tr (min) d (in) h (in) Lss SR

    SIZING

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process (Assu

    a CD = 0.34 ).

    = 0,0119

    .

    = 0,0049

    CD =24

    3

    . 0.34

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process

    (Assume a CD = 0.34 ).

    2. Calculate the capacity of the gas.

    21

    420

    m

    D

    gl

    gg

    eff

    d

    C

    P

    TZQdL

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process

    (Assume a CD = 0.34 ).

    2. Calculate the capacity of the gas.3. Calculate the capacity of the liquid.

    7,0

    2 lr

    eff

    Qt

    Ld

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process

    (Assume a CD = 0.34 ).

    2. Calculate the capacity of the gas.3. Calculate the capacity of the liquid.

    4. Establish relationships between the diameter of the spacer ( d

    and the effective length ( Leff ) capabilities for gas and liquid.

    d (in) Gas Leff(ft) Liquid Leff(ft)

    16

    20

    24

    30

    36

    42

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process (Ass

    CD = 0.34 ).

    2. Calculate the capacity of the gas.3. Calculate the capacity of the liquid.

    4. Establish relationships between the diameter of the spacer ( d

    the effective length ( Leff ) capabilities for gas and liquid.

    5. Calculate the length between weld beads (LSS ) for each diam

    12

    dLL effss 5,2 effss LL ss L

    4

    3

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process (Ass

    CD = 0.34 ).

    2. calculate the capacity of the gas.3. calculate the capacity of the liquid.

    4. Establish relationships between the diameter of the spacer ( d

    the effective length ( Leff ) capabilities for gas and liquid.

    5. Calculate the length between weld beads (LSS ) for each diam

    6. Determine the slenderness ratio for each diameter.

    d

    LSR SS

    12

    SEPARATORS

    DESING TWO-PHASESEPARATORS

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    1. Determine the drag coefficient CD by a iterative process (Ass

    CD = 0.34 ).

    2. Calculate the capacity of the gas.3. Calculate the capacity of the liquid.

    4. Establish relationships between the diameter of the spacer ( d

    the effective length ( Leff ) capabilities for gas and liquid.

    5. Calculate the length between weld beads (LSS ) for each diam

    6. Determine the slenderness ratio for each diameter.

    7. Select the option that contains a slenderness ratio between 3If two or more options are in that range, you can take the deci

    use smaller diameter , it implies a lower cost .

    SEPARATORS

    DESING TWO-PHASE VERTICALSEPARATORS

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    1. The first step in sizing a vertical separator is to establish the de

    basis. (CD)

    SYMBOL VALOR UNITS

    Qg 10 MMSCFD

    Qo 2000 BPD

    API 40

    P 1000 Psia

    T 60 F

    (SG)g 0,6

    Dm 140 Micras

    m 0,013 Cp

    Z 0,84

    Tr 3 min

    DESING TWO-PHASE VERTICALSEPARATORS

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    1. The first step in sizing a vertical separator is to establish the de

    basis. (CD)

    = ( ,

    ,+) = 2,7(

    )

    = 51,6 /3 = 3,71 /3

    DESING TWO-PHASE VERTICALSEPARATORS

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    2. Determine the drag coefficient CD by a iterative process (Assu

    CD = 0.34).

    CD =24

    = 0,0119

    .

    = 0,0049

    SYMBOL VALOR UNITS

    l 51,6 Lb/ft3

    g 3,7 Lb/ft3

    dm 140 Micras

    m 0,013 Cp

    CD 0,340 F

    Vt

    DESING TWO-PHASE VERTICALSEPARATORS

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    2. Determine the drag coefficient CD by a iterative process (Assu

    CD = 0.34).

    ITERATION Vt Re CD

    1 0,867 169,8 0,712

    2 0,600 117,3 0,821

    3 0,558 109,2 0,847

    4 0,550 107,6 0,852

    5 0,548 107,2 0,854

    DESING TWO-PHASE VERTICALSEPARATORS

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    3. Calculate d, may be used to determine the minimum rediameter. Any diameter larger than this value may be used.

    21

    420

    m

    D

    gl

    gg

    effd

    C

    P

    TZQdL

    indLeff 9,21

    DESING TWO-PHASE VERTICALSEPARATORS

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    4. For a selected d, may be used to determine h.

    5. From d and h, the seam-to-seam length may be estimate

    larger value of Lss should be used.

    7,0

    2 lreff

    QtLd =

    0,12

    =

    76

    12

    = 76

    12

    36

    36

    DESING TWO-PHASE VERTICALSEPARATORS

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    = (12

    )

    tr(min) d(in) h(in) Lss(ft) Sg

    1 24 28,9 8,7 4,4

    1 30 18,5 7,9 3,2

    1 36 12,9 7,4 2,5

    1 42 9,4 7,6 2,2

    1 48 7,2 7,9 2,0

    CONCLUSIONS

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    While designing the separators, it is essential to keep in

    pressure conditions, temperature as well as the properties obeing separated. This is in order to design the proper dimensi

    equipment.

    The horizontal separators have an are big enough which en

    existence of more equilibrium between the phases and enh

    liberation of gas towards the zone of the mist extractor.

    CONCLUSIONS

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    The design of the separators has the end goal of deter

    diameter and the optimal longitude, precise to the inch, in ord

    the retention time required making the process of separ

    efficient.

    BIBLIOGRAPHY

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    Arnold, K. Surface Production Operations. Volume II. Thir Editio

    M.Campbell. Gas conditioning and processing. Volume 2Equipment Modules. 1984.

    Gas Processors Suppleters Association. Engineering Data

    2004.